Aliphatic/Aromatic Petroleum Hydrocarbons in Soils by GCxGC-FID

SOP: 2680

UKAS accredited; MCERTS accredited

UKAS accredited: all bands  in the range C8–C40

MCERTS accredited: all bands in the range C8–C35

aliphatic banding: >C5–C6, >C6–C8,>C8–C10, >C10–C12, >C12–C16, >C16–C21, >C21– C35, >C35– C44

aromatics banding: >C5–C7, >C7–C8, >C8–C10, >C10–C12, >C12–C16, >C16– C21,  >C21– C35, >C35– C44

Methodology – Extraction of an as received soil sample, following chemical drying with sodium sulphate, into dichloromethane followed by determination of total petroleum hydrocarbons by two dimensional gas chromatography using flame ionisation detection (GCxGC-FID).

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